Portable XRD Analyzers

The TERRA Mobile XRD System, a high performing, completely contained, battery operated, closed-beam portable XRD, provides full phase ID of major, minor and trace components with a qualitative XRF scan of elements Ca - U. Its unique, minimal sample prep technique and sample chamber allow for fast, in-field analysis.

Overview

Patented Technology From NASA and Olympus

Initially conceived to perform chemical and mineralogical testing for NASA’s Mars Science Laboratory (MSL) mission, Olympus’ TERRA is a rugged, fully portable field instrument which harnesses advanced dual XRD/XRF technology and renders it for earthbound applications. Combining both Olympus and NASA innovation, TERRA brings to life a new way of performing X-ray diffraction and X-ray fluorescence measurements.

Using a specifically developed direct excitation charge coupled device (CCD) “camera”, TERRA is able to collect X-ray photon data for both X-ray diffraction and X-ray fluorescence simultaneously. This is the result of the integrated camera’s ability to detect both photon position and photon energy at the same time. With energy resolution of ~200 eV (5.9 keV), TERRA makes XRF analysis as simple as viewing the software spectrum display.

Easy Sample Preparation

Terra

TERRA radically simplifies sample collection for your X-ray diffraction experiments. Typically, a sample must be finely ground and pressed into a pellet in order to ensure a sufficiently random orientation of the crystals.

TERRA’s patented sample vibration chamber eliminates this issue. Requiring a mere 15 mg sample, the vibration chamber’s convection process presents the instrument optics with multifarious orientations of the crystalline structure. This results in a superb X-ray diffraction pattern, virtually free of the problematic preferred-orientation effects encountered when using classic preparation methods.

Due to its unique powder-handling system, nonmechanical goniometers, and lack of complicated moving parts, TERRA is extremely well suited for those applications where field portability and/or ease of use is at issue.

Software

X-ray Diffraction Data

X-ray Diffraction Data

Search/Match & XRD Quantitative Analysis Software Included

X-ray Fluorescence Data

X-ray Fluorescence Data

Qualitative XRF Scan

XPowder Software

TERRA is shipped with the necessary software (XPowder) for processing the resulting X-ray diffraction data. This includes the AMSCD mineral database.

For quantitative analysis, XPowder comes complete with reference intensity ratio (RIR) quantitative analysis methods as well as full-pattern analysis tools.

Furthermore, TERRA provides XRD pattern data in a variety of file formats, making XRD pattern interpretation in third-party programs easily accessible.

XPowder Software

Connectivity

TERRA operates off software embedded in the unit itself. The user accesses the operating system through a wireless connection (802.11b/g). This remote operation method allows for a wide degree of flexibility in controlling the instrument and subsequent data handling.

Specifications

XRD resolution0.25° 2θ FWHM
XRD range5-55° 2θ
Detector type1024 × 256 pixels - 2D Peltier-cooled CCD
XRF energy resolution250 eV at 5.9 keV
XRF energy range3 to 25 keV
Sample grain size<150 μm crushed minerals - (100 mesh screen, 150 μm)
Sample quantity~15 mg
X-ray target materialCu or Co (Cu standard)
X-ray tube voltage30 kV
X-ray tube power10 W
Data Storage40 GB - Ruggedized internal hard drive
Wireless Connectivity802.11b/g for remote control from web browser
Operating Temperature-10 °C to 35 °C
Weight14.5 kg with four batteries
Size48.5 cm × 39.2 cm × 19.2 cm (19.1 in. × 15.4 in. × 7.6 in.)
EnclosureIP67, MIL C-4150J rugged case
Field autonomy~4 hours (hot swap batteries)

Applications

Portable XRD/XRF has completely revolutionized geochemical exploration, mine grade control, metallurgical and process analysis, on-site HAZMAT inspections and in-field counterfeit pharmaceutical determinations. The TERRA's high quality data and speed of analysis delivers quantitative real-time compositional chemistry, right at the point of the sample location, where you need it most.

Mining & Ores

  • Calcite in Coal - Quantify calcite (CaCO3), a mineral identified as reducing the efficiency of the raw material fuel in a coal-fired plant, to improve efficiency and reduce carbon emissions
  • Potash - Analyze potash for phase identification and semiquantitative analysis of identified minerals such as sylvite, halite, langbenite and leonite. For further refinement, Sietronics Siroquant is available
  • Limestone & Cement - Easily perform quantitative analysis of common minerals associated with limestone - alpha-quartz, asbestos minerals, calcite, dolomite and more. In cases where the quarry contains various levels of dolomite, the TERRA quickly determines this mineral in the range of 0.50 to 9.0% with an error of only 0.02%.
Bring the Terra portable XRD system into the mine for real time mineralogy analysis.

Petrochemical

Mudlogging made easy using the Terra portable XRD system.
  • Mudlogging - Perform mineral ID and quantification on shale cuttings in the field for rapid feedback at drilling sites - simplify "chasing the vein" of a given mineral strata
  • Pipelines - TERRA Smart Sense allows optimum peak-to-background performance to identify and quantify corrosion materials on pipelines; simultaneous XRF measurements give rapid identification of elemental constituents
  • Easily reanalyze mine tailings to determine mill performance or evaluate historical projects

Fast HAZMAT ID

  • Rapidly ID dangerous hazardous materials on-site for local & global security
  • Identify explosives, fusing materials & accelerants on location
  • ID & quantify suspected hazardous materials: azide's PETN, black powder's KClO3, KClO4 & KNO3, flash powder's KClO3 & cascandite
security analysis using the Terra portable XRD system

Pharmaceuticals

detect counterfeit pharamceuticals using the Terra portable XRD system.
  • Rapid ID of counterfeit pharmaceuticals
  • Fast, non-destructive fingerprinting of drug formulations & precursors
  • Test for presence and quantity of active and inactive, foreign or substitute ingredients
  • Fast XRD screening ensures patient safety and safeguards legitimate pharmaceutical manufacturers' branding

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